Electron Paramagnetic Resonance Spectroscopy

University of Geneva - Switzerland

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  • Single Crystal EPR Studies of Radicals Produced by Radiolysis of Organophosphorus Compounds

    in "Applications of EPR in Radiation Research" Anders Lund - Masaru Shiotani Eds., Springer, (2014), p33-66
    DOI:10.1007/978-3-319-09216-4_2 | unige:42196


  • Role of the aromatic bridge on radical ions formation during reduction of diphosphaalkenes
    M. Lejeune, P. Grosshans, T. Berclaz, H. Sidorenkova, C. Besnard, P. Pattison and
    New Journal of Chemistry, 35 (11) (2011), p2510-2520
    DOI:10.1039/c1nj20314b | unige:17483 | Abstract | Article HTML | Article PDF


  • C 3 symmetric tris(phosphonate)-1,3,5-triazine ligand: homopolymetallic complexes and its radical anion
    C. Maxim, A. Matni, , M. Andruh, N.G.R. Hearns, R. Clérac and N. Avarvari
    New Journal of Chemistry, 34 (10) (2010), p2319-2327
    DOI:10.1039/C0NJ00204F | unige:14779 | Abstract | Article HTML | Article PDF
  • Bis(tetrathiafulvalenes) with aromatic bridges: electron delocalization in the oxidized species through EPR and theoretical studies
    F. Riobé, N. Avarvari, P. Grosshans, H. Sidorenkova, T. Berclaz and
    Physical Chemistry Chemical Physics, 12 (2010), p9650-9660
    DOI:10.1039/C001014F | unige:14784 | Abstract | Article HTML | Article PDF


  • The effect of electron-withdrawing groups in the fragmentation of the radical anions of benzyl phenyl ethers
    X. Asensio, A. González-Lafont, J. Marquet, J.M. Lluch and
    Journal of Molecular Structure: THEOCHEM, 913 (1-3) (2009), p928-935
    DOI:10.1016/j.theochem.2009.07.047 | unige:6176 | Article PDF
  • Rigid Bis(tetrathiafulvalenes) Doubly Bridged by Phosphino Groups and Derivatives: Synthesis and Intramolecular Mixed Valence State
    I. Danila, F. Biaso, H. Sidorenkova, , M. Fourmigué, E. Levillain and N. Avarvari
    Organometallics, 28 (13) (2009), p3691-3699
    DOI:10.1021/om900107y | unige:3551 | Abstract | Article HTML | Article PDF
  • Mono- and Bis(tetrathiafulvalene)-1,3,5-Triazines as Covalently Linked Donor-Acceptor Systems: Structural, Spectroscopic, and Theoretical Investigations
    F. Riobé, P. Grosshans, H. Sidorenkova, and N. Avarvari
    Chemistry - A European Journal, 15 (2) (2009), p380-387
    Keywords: charge transfer | donor-acceptor systems | EPR spectroscopy | nitrogen heterocycles | structure elucidation | tetrathiafulvalenes
    DOI:10.1002/chem.200801851 | unige:3558 | Abstract | Article HTML | Article PDF


  • Helicate Extension as a Route to Molecular Wires
    D. Schultz, F. Biaso, A. Rehaman Moughal Shahi, , K. Rissanen, L. Gagliardi, C.J. Cramer and J.R. Nitschke
    Chemistry - A European Journal, 14 (24) (2008), p7180-7185
    DOI:10.1002/chem.200800503 | unige:3184 | Abstract | Article HTML | Article PDF
  • [CpNi(diselenolene)] Neutral Radical Complexes: Electron Paramagnetic Resonance and Density Functional Theory Investigations
    P. Grosshans, P. Adkine, H. Sidorenkova, M. Nomura, M. Fourmigué and
    Journal of Physical Chemistry A, 112 (17) (2008), p4067-4073
    DOI:10.1021/jp800584v | unige:3574 | Abstract | Article HTML | Article PDF
  • Synthesis of a stable radical anion via the one electron reduction of a 1,1-bis-phosphinosulfide alkene derivative
    T. Cantat, F. Biaso, A. Momin, L. Ricard, , N. Mézailles and P. Le Floch
    ChemComm, (7) (2008), p874-876
    DOI:10.1039/b715380e | unige:42 | Abstract | Article HTML | Article PDF


  • Multifrequency EPR study of S = 1 vanadium (III) complexes with nitrogen containing ligands
    M. Brynda, B.S. Krishnamoorthy, , G. Aromi and J Krzystek
    Abstracts of Papers, 234th ACS National Meeting, Boston, MA, (2007)
  • ESR/DFT study of bis-iminophosphorane cation radicals
    A. Matni, L. Boubekeur, P. Grosshans, N. Mézailles, G. Bernardinelli, P. Le Floch and
    Magnetic Resonance in Chemistry, 45 (12) (2007), p1011-1017
    Keywords: ESR ; DFT ; 1H ; 14N ; 31P ; hyperfine structure ; spin delocalization ; bis-iminophosphoranes ; cation radical
    DOI:10.1002/mrc.2079 | unige:3578 | Abstract | Article PDF
  • Intramolecular Mixed-Valence State Through Silicon or Germanium Double Bridges in Rigid Bis(Tetrathiafulvalenes)
    F. Biaso, , E. Canadell, P. Auban-Senzier, E. Levillain, M. Fourmigué and N. Avarvari
    Chemistry - A European Journal, 13 (19) (2007), p5394-5400
    Keywords: conducting materials; EPR spectroscopy; main group elements; mixed-valent compounds; tetrathiafulvalenes
    DOI:10.1002/chem.200700237 | unige:3592 | Abstract | Article HTML | Article PDF


  • Neutral, Radical [CpNi(dithiolene)] Complexes with Flexible, Nonplanar Seven-Membered Rings: [CpNi{S2C2S2(CH2)2X}] (X = CH2, CF2, C=CH2, S, C=O)
    M. Nomura, , P. Adkine and M. Fourmigué
    European Journal of Inorganic Chemistry, 2006 (24) (2006), p5012-5021
    Keywords: nickel ; S ligands ; radicals ; metallacycles ; magnetic properties
    DOI:10.1002/ejic.200600649 | unige:3634 | Abstract | Article HTML | Article PDF
  • [CpNi(dithiolene)] (and Diselenolene) Neutral Radical Complexes
    M. Nomura, T. Cauchy, , P. Adkine and M. Fourmigué
    Inorganic Chemistry, 45 (20) (2006), p8194-8204
    DOI:10.1021/ic0608546 | unige:3639 | Abstract | Article HTML | Article PDF
  • EPR and DFT Studies of the Structure of Phosphinyl Radicals Complexed by a Pentacarbonyl Transition Metal
    B. Ndiaye, S. Bhat, A. Jouaiti, T. Berclaz, G. Bernardinelli and
    Journal of Physical Chemistry A, 110 (31) (2006), p9736-9742
    DOI:10.1021/jp061960w | unige:3298 | Abstract | Article HTML | Article PDF
  • EPR and DFT studies of the one-electron reduction product of phospholium cations
    P. Adkine, T. Cantat, E. Deschamps, L. Ricard, N. Mézailles, P. Le Floch and
    Physical Chemistry Chemical Physics, 8 (2006), p862-868
    DOI:10.1039/b513736p | unige:3632 | Abstract | Article HTML | Article PDF
  • Chromium tricarbonyl complex of phosphaalkene: Crystal structure and electrochemistry of the Cr(CO)3 complex of PhC(H)=PMes*, EPR and DFT studies of its radical anion
    C. Gouverd, M. Brynda, T. Berclaz and
    Journal of Organometallic Chemistry, 691 (1-2) (2006), p72-78
    DOI:10.1016/j.jorganchem.2005.08.045 | unige:3288 | Abstract | Article HTML | Article PDF


  • Using the Diphosphanyl Radical as a Potential Spin Label: Effect of Motion on the EPR Spectrum of an R1(R2)P--PR1 Radical
    L. Cataldo, C. Dutan, S.K. Misra, S. Loss, H. Grützmacher and
    Chemistry - A European Journal, 11 (11) (2005), p3463-3468
    Keywords: EPR spectroscopy; internal rotation; phosphorus; radicals; spin labeling
    DOI:10.1002/chem.200401276 | unige:3277 | Abstract | Article PDF
  • Synthesis and X-ray Crystal Structure of a Cationic Homoleptic (SPS)2Rh(III) Complex and EPR Study of Its Reduction Process
    M. Doux, N. Mézailles, L. Ricard, P. Le Floch, P. Adkine, T. Berclaz and
    Inorganic Chemistry, 44 (4) (2005), p1147-1152
    DOI:10.1021/ic049046+ | unige:3627 | Abstract | Article HTML | Article PDF
  • Tetrathiafulvalene-phosphine-based iron and ruthenium carbonyl complexes: Electrochemical and EPR studies
    C. Gouverd, F. Biaso, L. Cataldo, T. Berclaz, , E. Levillain, N. Avarvari, M. Fourmigué, F.X. Sauvage and C. Wartelle
    Physical Chemistry Chemical Physics, 7 (2005), p85-93
    DOI:10.1039/b409958c | unige:3282 | Abstract | Article HTML | Article PDF


  • Effect of Conformational Changes on a One-Electron Reduction Process: Evidence of a One-Electron PP Bond Formation in a Bis(phosphinine)
    S. Choua, C. Dutan, L. Cataldo, T. Berclaz, , N. Mézailles, A. Moores, L. Ricard and P. Le Floch
    Chemistry - A European Journal, 10 (16) (2004), p4080-4090
    Keywords: aromaticity; density functional calculations; electron transfer; EPR spectroscopy; fluxionality; P ligands
    DOI:10.1002/chem.200400073 | unige:3252 | Abstract | Article HTML | Article PDF


  • Kinetic Stabilization of Primary Hydrides of Main Group Elements. The Synthesis of an Air-Stable, Crystalline Arsine and Silane
    M. Brynda, G. Bernardinelli, C. Dutan and
    Inorganic Chemistry, 42 (21) (2003), p6586-6588
    DOI:10.1021/ic034367r | unige:3508 | Abstract | Article HTML | Article PDF
  • Sterically Encumbered Diphosphaalkenes and a Bis(diphosphene) as Potential Multiredox-Active Molecular Switches: EPR and DFT Investigations
    C. Dutan, S. Shah, R.C. Smith, S. Choua, T. Berclaz, and J.D. Protasiewicz
    Inorganic Chemistry, 42 (20) (2003), p6241-6251
    DOI:10.1021/ic030079j | unige:3507 | Abstract | Article HTML | Article PDF
  • Phosphaalkenes with Inverse Electron Density: Electrochemistry, Electron Paramagnetic Resonance Spectra, and Density Functional Theory Calculations of Aminophosphaalkene Derivatives
    P. Rosa, C. Gouverd, G. Bernardinelli, T. Berclaz and
    Journal of Physical Chemistry A, 107 (24) (2003), p4883-4892
    DOI:10.1021/jp030023a | unige:3239 | Abstract | Article HTML | Article PDF
  • Electron transfer between two sylil-substituted phenylene rings: EPR/ENDOR spectra, DFT calculations, and crystal structure of the one-electron reduction compound of a di(m-silylphenylenedisiloxane)
    C. Dutan, S. Choua, T. Berclaz, , N. Mézailles, A. Moores, L. Ricard and P. Le Floch
    Journal of the American Chemical Society, 125 (15) (2003), p4487-4494
    DOI:10.1021/ja0209060 | unige:3243 | Abstract | Article HTML | Article PDF
  • Intramolecular motion in the triptycenegermanyl radical: single crystal EPR study at variable temperature and DFT calculations
    M. Brynda, C. Dutan, T. Berclaz, and G. Bernardinelli
    Journal of Physics and Chemistry of Solids, 64 (6) (2003), p939-946
    Keywords: organic compounds; EPR; molecular dynamics; quantum chemical method
    DOI:10.1016/S0022-3697(02)00452-3 | unige:3611 | Abstract | Article HTML | Article PDF


  • Formation and structure of Rh(0) complexes of phosphinine-containing macrocycles: EPR and DFT investigations
    L. Cataldo, S. Choua, T. Berclaz, , N. Mézailles, N. Avarvari, F. Mathey and P. Le Floch
    Journal of Physical Chemistry A, 106 (12) (2002), p3017-3022
    DOI:10.1021/jp014339z | unige:3227 | Abstract | Article HTML | Article PDF
  • Electron Paramagnetic Resonance, Optimization and Automatic Differentiation
    E.J. Soulié, C. Faure, T. Berclaz and
    in "Automatic Differentiation of Algorithms" Springer, New-York, (2002), p99-106
  • Characterization of transient radicals in the reduction product of the -P=C=C=P- system: EPR and theoretical studies
    H. Sidorenkova, M. Chentit, S. Choua, and Y. Ellinger
    Physical Chemistry Chemical Physics, 4 (20) (2002), p4931-4936
    DOI:10.1039/b205848k | unige:3608 | Abstract | Article HTML | Article PDF
  • Dynamic phenomena in barrelenephosphinyl radicals: a complementary approach by density matrix analysis of EPR spectra and DFT calculations
    M. Brynda, C. Dutan, T. Berclaz and
    Current Topics in Biophysics, 26 (1) (2002), p35-42


  • Formation of a phosphorus-phosphorus bond by successive one-electron reductions of a two-phosphinines-containing macrocycle: Crystal structures, EPR and DFT investigations
    L. Cataldo, S. Choua, T. Berclaz, , N. Mézailles, L. Ricard, F. Mathey and P. Le Floch
    Journal of the American Chemical Society, 123 (27) (2001), p6654-6661
    DOI:10.1021/ja010331r | unige:3220 | Abstract | Article HTML | Article PDF
  • EPR and theoretical studies of the reduction product of the fulvenephosphaallene system
    M. Chentit, H. Sidorenkova, S. Choua, , Y. Ellinger and G. Bernardinelli
    Journal of Organometallic Chemistry, 634 (2) (2001), p136-144
    Keywords: phosphaallenes; EPR; DFT; radical anion; phosphaallylic radical
    DOI:10.1016/S0022-328X(01)01098-1 | unige:3606 | Abstract | Article PDF


  • One-electron reduction product of biphosphinine derivative and of its Ni(0) complex: crystal structure, EPR/ENDOR and DFT investigations on (tmbp).- and [Ni(tmbp)2].-
    S. Choua, H. Sidorenkova, T. Berclaz, , P. Rosa, N. Mézailles, L. Ricard, F. Mathey and P. Le Floch
    Journal of the American Chemical Society, 122 (49) (2000), p12227-12234
    DOI:10.1021/ja002125+ | unige:3604 | Abstract | Article HTML | Article PDF

  • Role of hydroxyl radicals and singlet oxygen in the formation of primary radicals in unsaturated lipids: A solid state Electron Paramagnetic Resonance study
    , P. Lambelet and P. Richert
    Journal of Agricultural and Food Chemistry, 48 (4) (2000), p974-978
    DOI:10.1021/jf990684y | unige:3206 | Abstract | Article HTML | Article PDF


  • Spin labeled hydroxyproline analogues
    J.M.J. Tronchet, C. Jorand, G. Zosimo-Landolfo and
    Il Farmaco, 54 (1999), p637-641
    Keywords: L-Proline; N-hydroxyamino; EPR spectroscopy; aminoxyls
    DOI:10.1016/S0014-827X(99)00083-X | unige:2733 | Abstract | Article HTML | Article PDF
  • EPR/ENDOR study of an X-irradiated single crystal of 1-triphenylphosphoranylidene-2-propanone : the role of hydrogen bonds in the trapping of radiogenic radical
    T. Berclaz, G. Bernardinelli, , G. Rao and Z. Tancic
    Radiation physics and chemistry, 56 (5-6) (1999), p539-545
    DOI:10.1016/S0969-806X(99)00295-9 | unige:2736 | Abstract | Article HTML | Article PDF
  • Air-stable crystalline primary phosphines and germanes : synthesis and crystal structures of dibenzobarellenephosphine and tribenzobarellenegermane
    M. Brynda, and G. Bernardinelli
    ChemComm, (11) (1999), p961-962
    DOI:10.1039/a901083a | unige:2735 | Abstract | Article PDF
  • An EPR/ENDOR study of the reduction products of symmetrical isomers of dipyridylacetylene
    S. Choua, A. Jouaiti and
    Physical chemistry chemical physics, 1 (15) (1999), p3557-3560
    DOI:10.1039/a902689d | unige:2737 | Abstract | Article PDF
  • Bicyclonucleosides and ring-chain interconversion
    J.M.J. Tronchet, M. Zsély, L. Brenas, O. Lassout, E. Grand, P. Seuret, M. Grigorov, E. Rivara-Minten and
    Nucleosides, Nucleotides and Nucleic Acids, 18 (4&5) (1999), p1077-1078
    DOI:10.1080/15257779908041651 | unige:2749 | Abstract | Article PDF


  • Synthesis and conformational analysis of a novel type of spin labelled bicyclonucleoside based on a tetrahydrofurano(2,3-c)pyrrolidine sugar skeleton
    J.M.J. Tronchet, L. Brenas, F. Barbalat-Rey, M. Zsély and
    Nucleosides, Nucleotides and Nucleic Acids, 17 (6) (1998), p1019-1031
    DOI:10.1080/07328319808004218 | unige:2765 | Abstract | Article PDF
  • Hindered rotation around a C-.PH bond A single-crystal EPR study of the diphenyldibenzobarrelenephosphinyl radical
    M. Brynda, T. Berclaz, , G. Ramakrishnan and G. Bernardinelli
    Journal of Physical Chemistry A, 102 (43) (1998), p8245-8250
    DOI:10.1021/jp9816519 | unige:2766 | Abstract | Article HTML | Article PDF
  • Reduction of monophosphaallenes: An EPR study and ab inition investigations of (HPCCH2)-. and (HPCHCH2). radicals
    M. Chentit, H. Sidorenkova, and Y. Ellinger
    Journal of Physical Chemistry A, 102 (51) (1998), p10469-10475
    DOI:10.1021/jp982519b | unige:2767 | Abstract | Article HTML | Article PDF
  • Spin labelled dinucleosides
    J.M.J. Tronchet, E. Grand, M. Zsély, R. Giovannini and
    Carbohydrate Letters, 3 (3) (1998), p161-168
  • Blocked sugar analogues bearing two or three N(sp3)-= bonds
    J.M.J. Tronchet, M. Koufaki, F. Barbalat-Rey and
    Carbohydrate Letters, 3 (4) (1998), p255-262
  • Electron Paramagnetic Resonance studies of radicals and ions with a low-coordinated phosphorus atom

    Recent research developments in physical chemistry, 2 (4) (1998), p311-321


  • Di-[mu]-bromo-bis{[(2,4,6-tris-tert-butyl-phenyl)phosphanediylmethyl-P]phenyl-C2}-dipalladium
    M. Chentit, and G. Bernardinelli
    Acta Crystallographica C, 53 (1997), p866-868
    DOI:10.1107/S0108270197003235 | unige:2782 | Article PDF
  • Spin labelled 2',3'-seconucleoside derivatives
    J.M.J. Tronchet, M. Zsély, D. Cabrini, F. Barbalat-Rey, N. Dolatshahi and
    Carbohydrate Letters, 2 (1997), p389-394
  • Phosphaalkene derivatives of furane and thiophene : synthesis, crystal structure, electrochemistry and EPR study of their radical anions
    A. Jouaiti, A. Al Badri, and G. Bernardinelli
    Journal of Organometallic Chemistry, 529 (1-2) (1997), p143-149
    Keywords: phosphaalkene; electron spin resonance; electrochemistry; crystal structure; radical anion
    DOI:10.1016/S0022-328X(96)06526-6 | unige:2807 | Abstract | Article PDF
  • The structure of diphosphaallenic radical cations as evidenced by EPR experiments and ab initio calculations
    M. Chentit, H. Sidorenkova, A. Jouaiti, G. Terron, and Y. Ellinger
    Journal of the Chemical Society. Perkin transactions 2, 1997 (5) (1997), p921-926
    unige:2808 | Abstract | Article PDF
  • Radiation damage in Pt(II) complexes : EPR study of an x-irradiated single crystal of Pt(1,3-dimethyl.imidazoline-2-thione)4Cl2.4H2O
    M. Wermeille, , S. Misra, P. Arrizabalaga and G. Bernardinelli
    Radiation Physics and Chemistry, 49 (3) (1997), p347-356
    DOI:10.1016/S0969-806X(96)00146-6 | unige:2809 | Abstract | Article PDF


  • ENDOR spectra of an X-irradiated single crystal of the R3P=CH-C(O)CH3 Wittig reagent
    T. Berclaz, , G. Rao and Z. Tancic
    Bulletin of Magnetic Resonance, 17 (1-4) (1996), p296-297
  • Synthesis and characterisation of a heterodinuclear ruthenium(II)-palladium(II) complex with two different cyclometallating sites
    A. Jouaiti, and J.-P. Collin
    Inorganica Chimica Acta, 245 (1) (1996), p69-73
    Keywords: ruthenium complexes | palladium complexes | cyclometallated ligand complexes | heterodinuclear complexes
    DOI:10.1016/0020-1693(95)04799-9 | unige:2819 | Abstract | Article PDF
  • Nucleosides and acyclonucleosides bearing a N-hydroxyureido group
    J.M.J. Tronchet, M. Zsély, M. Iznaden, F. Barbalat-Rey, and G. Bernardinelli
    Carbohydrate letters, 2 (1996), p101-108
  • 1,2-Bis[2,4,6-tri-tert-butylphenyl]phosphanediylmethyl]benzene, L : synthesis and structure of L, of the chelated complex [PdLCl2] and of a derived cyclometallated chiral complex
    A. Jouaiti, and G. Bernardinelli
    ChemComm, (3) (1996), p437-438
    DOI:10.1039/CC9960000437 | unige:2838 | Abstract | Article PDF
  • 9-substituted triptycene as a probe for the study of internal rotation around a C-PH bond in the solid state : a single crystal EPR study at variable temperature
    G. Ramakrishnan, A. Jouaiti, and G. Bernardinelli
    Journal of Physical Chemistry, 100 (26) (1996), p10861-10868
    DOI:10.1021/jp960836h | unige:2835 | Abstract | Article HTML | Article PDF


  • Synthesis of 3-aza-8-oxabicyclo[3.3.0]octane and 3-aza-9-oxabicyclo[4.3.0]nonane derivatives from D-glucose via retro-cope eliminations
    J.M.J. Tronchet, M. Zsély, R.N. Yazji, F. Barbalat-Rey and
    Carbohydrate letters, 1 (1995), p343-348
  • Spin-labelled glycolipid analogues : D-glucose series
    J.M.J. Tronchet, M. Zsély and
    Carbohydrate Research, 275 (2) (1995), p245-258
    DOI:10.1016/0008-6215(95)00177-U | unige:2843 | Abstract | Article PDF
  • Spin labelled C-glycoside analogs : derivatives of 1,4-anhydro-4-deoxy-2,3-O-cyclopentylidene-1,4-N-hydroxyimino-DL-erythrofuranose
    J.M.J. Tronchet, M. Balkadjian, G. Zosimo-Landolfo, F. Barbalat-Rey, P. Lichtle, A. Ricca, I. Komaromi, G. Bernardinelli and
    Journal of Carbohydrate Chemistry, 14 (1) (1995), p17-34
    DOI:10.1080/07328309508006434 | unige:2844 | Abstract | Article PDF
  • Oxidation of a tricoordinated Cu-I complex to a tetracoordinated Cu-II species : a single-crystal EPR study
    C. Palivan, T. Berclaz, , S. Ramaprabhu and G. Bernardinelli
    Journal of the Chemical Society. Faraday transactions, 91 (14) (1995), p2155-2160
    DOI:10.1039/FT9959102155 | unige:2858 | Abstract | Article PDF
  • The benzodiphosphaalkene ligand and its Pd-II and Pt-II complexes : their synthesis, structure and an ESR study of their reduction products
    A. Jouaiti, , G. Terron and G. Bernardinelli
    Journal of the American Chemical Society, 117 (8) (1995), p2251-2258
    DOI:10.1021/ja00113a014 | unige:2849 | Abstract | Article PDF
  • Radical reactions in a single crystal of phosphaalkene: EPR and ab initio calculations of phosphoniumyl radical cations
    S.N. Bhat, T. Berclaz, and A. Jouaiti
    Journal of Physical Chemistry, 99 (43) (1995), p15864-15869
    DOI:10.1021/j100043a026 | unige:2853 | Abstract | Article PDF
  • Anhydrous Form of Carnidazole, C8H12N4O3S
    G. Bernardinelli, T. Berclaz, and N. Rajalakshmi
    Acta Crystallographica C, 51 (7) (1995), p1390-1392
    DOI:10.1107/S0108270195000217 | unige:2854 | Abstract | Article PDF

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